Fe₂O₃ PARTICLES AS PRECURSORS FOR α”-Fe₁₆N₂ PHASE SYNTHESIS

Authors

  • R. A. ONE Babeş-Bolyai University, Faculty of Physics, Cluj-Napoca, Romania. corresponding author: sever.mican@phys.ubbcluj.ro
  • R. BORTNIC Babeş-Bolyai University, Faculty of Physics, Cluj-Napoca, Romania. corresponding author: sever.mican@phys.ubbcluj.ro https://orcid.org/0000-0003-2844-8950
  • S. MICAN Babeş-Bolyai University, Faculty of Physics, Cluj-Napoca, Romania. corresponding author: sever.mican@phys.ubbcluj.ro https://orcid.org/0000-0002-7186-5883
  • Lucian BARBU-TUDORAN National Institute for R&D of Isotopic and Molecular Technologies, Cluj-Napoca, Romania. corresponding author: lucian.barbu@itim-cj.ro https://orcid.org/0000-0003-0360-016X
  • V. POP Babeş-Bolyai University, Faculty of Physics, Cluj-Napoca, Romania. corresponding author: viorel.pop@phys.ubbcluj.ro https://orcid.org/0000-0001-5125-4412

Keywords:

Hematite, Sol-gel synthesis, Shape anisotropy, X-ray Diffraction, Calorimetry, Annealing.

Abstract

In this work we investigate the structural properties and microstructure of Fe2O3 particles synthesized using the sol-gel method. Differential thermal and thermogravimetric analysis showed that the organic matrix is completely burned off at temperatures higher than 520 °C. The sample annealed at 550 °C for 12 h contained only the Fe2O3 phase. The obtained hematite particles are micrometer sized and have an elongated shape. Taking into account the cheap and available sol-gel precursors, the possibility of using these particles in α”-Fe16N2 synthesis is discussed.

Author Biographies

R. A. ONE, Babeş-Bolyai University, Faculty of Physics, Cluj-Napoca, Romania. corresponding author: sever.mican@phys.ubbcluj.ro

Babeş-Bolyai University, Faculty of Physics, 1 M. Kogălniceanu, 400084 Cluj-Napoca, Romania.

corresponding author: sever.mican@phys.ubbcluj.ro

R. BORTNIC, Babeş-Bolyai University, Faculty of Physics, Cluj-Napoca, Romania. corresponding author: sever.mican@phys.ubbcluj.ro

Babeş-Bolyai University, Faculty of Physics, 1 M. Kogălniceanu, 400084 Cluj-Napoca, Romania.

corresponding author: sever.mican@phys.ubbcluj.ro

S. MICAN, Babeş-Bolyai University, Faculty of Physics, Cluj-Napoca, Romania. corresponding author: sever.mican@phys.ubbcluj.ro

Babeş-Bolyai University, Faculty of Physics, 1 M. Kogălniceanu, 400084 Cluj-Napoca, Romania. corresponding author: sever.mican@phys.ubbcluj.ro

Lucian BARBU-TUDORAN, National Institute for R&D of Isotopic and Molecular Technologies, Cluj-Napoca, Romania. corresponding author: lucian.barbu@itim-cj.ro

National Institute for R&D of Isotopic and Molecular Technologies, 75-103 Donath, 400293, Cluj-Napoca, Romania. corresponding author: lucian.barbu@itim-cj.ro

V. POP, Babeş-Bolyai University, Faculty of Physics, Cluj-Napoca, Romania. corresponding author: viorel.pop@phys.ubbcluj.ro

Babeş-Bolyai University, Faculty of Physics, 1 M. Kogălniceanu, 400084 Cluj-Napoca, Romania. corresponding author: viorel.pop@phys.ubbcluj.ro

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STUDIA UBB PHYSICA, Volume 61 (LXI), No. 1, June, 2016

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Published

2016-06-30

How to Cite

ONE, R. A., BORTNIC, R., MICAN, S., BARBU-TUDORAN, L., & POP, V. (2016). Fe₂O₃ PARTICLES AS PRECURSORS FOR α”-Fe₁₆N₂ PHASE SYNTHESIS. Studia Universitatis Babeș-Bolyai Physica, 61(1), 93–98. Retrieved from http://193.231.18.162/index.php/subbphysica/article/view/5818

Issue

Volume 61, No. 1, 2016

Section

Articles

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Copyright (c) 2016 Studia Universitatis Babeș-Bolyai Physica

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