SYNTHESIS AND PRELIMINARY CHARACTERIZATION OF MODIFIED 45S5 BIOGLASSES

Authors

  • S. IONITA Faculty of Physics, Alexandru Ioan Cuza University, Iasi, Romania
  • K. MAGYARI Interdisciplinary Research Institute on Bio-Nano-Sciences, Babes-Bolyai University, Cluj-Napoca, Romania https://orcid.org/0000-0003-1770-8454
  • A.V. SANDU Faculty of Materials Science and Engineering, Gheorghe Asachi Technical University, Iaşi, Romania https://orcid.org/0000-0002-9292-749X
  • V. SIMON Faculty of Physics & Interdisciplinary Research Institute on Bio-Nano-Sciences, Babes-Bolyai University, 400084 Cluj-Napoca, Romania
  • F. IACOMI Faculty of Physics, Alexandru Ioan Cuza University, Iasi, Romania. * Corresponding author: iacomi@uaic.ro https://orcid.org/0000-0001-7952-3741

DOI:

https://doi.org/10.24193/subbphys.2020.03

Keywords:

bioglasses; sol-gel-synthesis; XRD; SEM; EDX.

Abstract

The study is devoted to synthesis and preliminary structural and morphological characterization of modified 45S5 glasses, in (66-x)SiO2∙27CaO∙4P2O5∙3TiO2∙xAl2O3 system, with potential applications in dentistry. The composition of the sol-gel derived samples was verified with respect to their nominal composition. The effect of partial SiO2 replacement with Al2O3 on samples structure and morphology is investigated. It was established that the Ca/P ratio is diminished in Al2O3 containing samples and that an amorphous hydroxyapatite phase similar to hydroxyapatite reported for bone tissue is formed.

References

D. Ksouri, H. Khireddine, A. Aksas, T. Valente, F. Bir, N. Slimani, B. Cabal, R. Torrecillas, J. D. Santos, NovaBiotechnol Chim 17(2), 150(2018).

R. A. Jalil, K. A. Matori, M. H. M. Zaid, N. Zainuddin, M. Z. A. Khiri, N. A. A. Rahman, W. N. W. Jusoh, E. Kul, J. Spetrosc.(Hindawi) 9170412 (2020).

N. Kourkoumelis, I. Balatsoukas, M. Tzaphlidou, J Biol Phys., 38(2), 279 (2012).

H. Zhang, B.W. Darvell, Acta Biomaterialia, 6 (8), 3216 (2010).

T. Kokubo, H. Takadama, Biomater., 27, 2907 (2006).

D. Bellucci, A.Sola, R. Salvatori, A. Anesi, L. Chiarini, V. Cannillo, Mater. Sci. Eng. C, 43, 573 (2014).

D. Bellucci, A. Sola, M. Gazzarri, F. Chiellini, V. A. Cannillo, Mater. Sci. Eng. C, 33, 1091 (2013).

K. Magyari, R. Stefan, D.C. Vodnar, A. Vulpoi, L. Baia, J. Non-Crystal. Solids 402, 182 (2014).

K. Magyari, R. One, I.-S. Todor, M. Baia, V. Simon, S. Simon, L. Baia, J. Raman Spectrosc. 47, 1102 (2016).

M. Tamasan, H. Szilagyi, E. Vanea, V. Simon, J. Optoelectron. Adv. M. 15, 879 (2013).

J. R. Jones, Acta Biomater. 9, 4457 (2013).

E.A. Abou Neel, D.M. Pickup, S.P. Valappil, R.J. Newport, J.C. Knowles, J. Mater. Chem., 19, 690 (2009).

L.L. Hench, J.M. Polak, Science, 295, 1014(2002).

L. L. Hench, J. Am. Ceram. Soc., 74, 1487 (1991).

T. Kokubo, Biomaterials; 12, 155 (1991).

Carta D, Knowles JC, Smith ME, Newport RJ, J Non-Cryst Solids, 353, 1141 (2007).

P. Kiran, V. Ramakrishna, M. Trebbin, N.K. Udayashankar, H.D. Shashikala, J. Adv. Res., 8, 279 (2017).

M. Taherian, R. Roaeeb, M. Fathi, M. Tamizifar, J. Adv. Ceram. 3(3), 207 (2014).

D. Ksouri, H. Khireddine, A. Aksas, T. Valente, F. Bir, N. Slimani, B. Cabal, R. Torrecillas, J. D. Santos, Nova Biotechnol Chim 17(2), 150 (2018).

L. Baia, M. Baia, W. Kiefer, J. Popp, S. Simon, Chem. Phys., 327, 63 (2006).

O. Kaygili, Tatar, Y. S. Keser, J. Sol-Gel Sci. Technol. 65,105 (2013).

STUDIA UBB PHYSICA, Volume 65 (LXV), No. 1-2, December 2020

Downloads

Published

2020-12-30

How to Cite

IONITA, S., MAGYARI, K., SANDU, A., SIMON, V., & IACOMI, F. (2020). SYNTHESIS AND PRELIMINARY CHARACTERIZATION OF MODIFIED 45S5 BIOGLASSES. Studia Universitatis Babeș-Bolyai Physica, 65(1-2), 19–25. https://doi.org/10.24193/subbphys.2020.03

Issue

Volume 65, No. 1-2, 2020

Section

Articles

License

Copyright (c) 2020 Studia Universitatis Babeș-Bolyai Physica

Creative Commons License

This work is licensed under a Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International License.